Synchronous second-derivative fluorimetric determination of carbaryl and 1-naphthol using solid-phase extraction.
نویسندگان
چکیده
منابع مشابه
Simultaneous determination of carbaryl and 1-naphthol by first-derivative synchronous non-protected room temperature phosphorescence.
The applicability of non-protected room temperature phosphorescence (NP-RTP) in real samples was demonstrated in the present work. In this methodology, only two reagents, potassium iodide and sodium sulfite, were used to obtain phosphorescent signals. Overlapping of the phosphorescence spectra was resolved by using first-derivative synchronous phosphorimetry. The synchronous first-derivative sp...
متن کاملSynchronous-derivative phosphorimetric determination of 1- and 2-naphthol in irrigation water by employing beta-cyclodextrin.
A room-temperature phosphorimetric (RTP) study of the inclusion process between 1- and 2-naphthol, beta-cyclodextrin (beta-CD) and 3-bromo-1-propanol as heavy atom pertuber has been performed. Experimental conditions were optimized for the formation of trimolecular complexes with lifetimes of 10.82 and 9.41 ms for 1- and 2-naphthol, respectively. A synchronous-derivative room-temperature phosph...
متن کاملSolid-phase extraction derivative aromatic compounds in water samples and determination of using GC-FID
A simple method to pre-concentrated derivative aromatic compounds on active carbon in column has been applied as stationary phase which is used to measure the concentration of derivative aromatic compounds in water samples by means of solid-phase extraction. To measure 250 cc water samples and 250mg active carbon could be applied. Next step is to measure the derivative aromatic compounds by inj...
متن کاملMicellar Liquid Chromatographic Determination of Carbaryl and 1-Naphthol in Water, Soil, and Vegetables
A liquid chromatographic procedure has been developed for the determination of carbaryl, a phenyl-N-methylcarbamate, and its main metabolite 1-naphthol, using a C18 column (250 mm × 4.6 mm) with a micellar mobile phase and fluorescence detection at maximum excitation/emission wavelengths of 225/333 nm, respectively. In the optimization step, surfactants sodium dodecyl sulphate (SDS), Brij-35 ...
متن کاملSolid Phase Extraction Using Modified Magnetic Iron Oxide Nanoparticles for Extraction and Spectrofluorimetric Determination of Carvedilol in Human Plasma Samples
A new analytical approach was developed involving magnetic solid–phase extraction and spectrofluorimetric determination of carvedilol in human plasma samples. A plasma sample was prepared and adjusted to pH 8.2–10, then carvedilol was quickly extracted using iron oxide magnetic nanoparticles modified by the surfactant cetyltrimethylammonium bromide and determined to apply spectrofluorimetry...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: BUNSEKI KAGAKU
سال: 1999
ISSN: 0525-1931
DOI: 10.2116/bunsekikagaku.48.841